{"id":2573,"date":"2017-11-16T12:18:22","date_gmt":"2017-11-16T11:18:22","guid":{"rendered":"http:\/\/www.pica-berlin.de\/?p=2573\/"},"modified":"2017-11-22T17:53:56","modified_gmt":"2017-11-22T16:53:56","slug":"high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils","status":"publish","type":"post","link":"https:\/\/www.pica-berlin.de\/en\/news\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\/","title":{"rendered":"high speed method for the determination of more than 700 pesticides in fat and oils"},"content":{"rendered":"

The conventional method of determining pesticides in fats and oils (\u00a764 LFGB-Method Collection) L00.00-34) uses a complicated procedure to separate the pesticide molecules from the fat molecules. It is known as GPC (Gel Permeation Chromatography).\u00a0 After that, the large volume of solvent is reduced in a vacuum to less than one milliliter.\u00a0 This method was developed in the 1980s and is still in use today in residue laboratories.<\/p>\n

\"\"<\/p>\n

PICA Method\u00a0\u00a0\u00a0<\/span>\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0\u00a0 Conventional Method<\/span><\/p>\n

 <\/p>\n

The time needed for the measurements that follow in the latest measurement system UHPLC-MSMS and GC-MSMS can also be reduced by optimizing the measurement parameters.<\/p>\n

 <\/p>\n

With this procedure we can offer an express screening analysis for pesticides in fats and oils (same day, one day, two days).<\/p>\n

 <\/p>\n

Our procedure is validated for an oil mixed matrix made up of raw soy bean, olive, sunflower seed and sesame oils. The quality and correctness of the method have been 100% confirmed in annual FAPAS ring tests since it was developed in 2015 (see\u00a0 table). The method has has also been successfully tested with fish oils and other animal fats such as milk fat.<\/p>\n

 <\/p>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
\n

ring test\/ compound<\/span><\/b><\/p>\n<\/td>\n

\n

rape seed oil-FAPAS_05107_09\/10-2015<\/span><\/b><\/p>\n<\/td>\n

\n

palm oil-FAPAS_04\/06-2016<\/span><\/b><\/p>\n<\/td>\n<\/tr>\n

\n

Aldrin<\/span><\/b><\/p>\n<\/td>\n

\n

\u221a<\/span><\/p>\n<\/td>\n

<\/td>\n<\/tr>\n
\n

gamma-HCH (Lindan)<\/span><\/b><\/p>\n<\/td>\n

\n

\u221a<\/span><\/p>\n<\/td>\n

<\/td>\n<\/tr>\n
\n

Nirofen<\/span><\/b><\/p>\n<\/td>\n

\n

\u221a<\/span><\/p>\n<\/td>\n

<\/td>\n<\/tr>\n
\n

PCB 153<\/span><\/b><\/p>\n<\/td>\n

\n

\u221a<\/span><\/p>\n<\/td>\n

<\/td>\n<\/tr>\n
\n

p,p\u00b4-DDE<\/span><\/b><\/p>\n<\/td>\n

\n

\u221a<\/span><\/p>\n<\/td>\n

<\/td>\n<\/tr>\n
\n

Cypermethrin<\/span><\/b><\/p>\n<\/td>\n

<\/td>\n\n

\u221a<\/span><\/p>\n<\/td>\n<\/tr>\n

\n

Endosulfan-alpha<\/span><\/b><\/p>\n<\/td>\n

<\/td>\n\n

\u221a<\/span><\/p>\n<\/td>\n<\/tr>\n

\n

Ethylparathion<\/span><\/b><\/p>\n<\/td>\n

<\/td>\n\n

\u221a<\/span><\/p>\n<\/td>\n<\/tr>\n

\n

Lambda-Cyhalothrine<\/span><\/b><\/p>\n<\/td>\n

<\/td>\n\n

\u221a<\/span><\/p>\n<\/td>\n<\/tr>\n

\n

p,p\u00b4-DDT<\/span><\/b><\/p>\n<\/td>\n

<\/td>\n\n

\u221a<\/span><\/p>\n<\/td>\n<\/tr>\n

\n

Erfolgsquote (%)<\/span><\/b><\/p>\n<\/td>\n

\n

100<\/span><\/p>\n<\/td>\n

\n

100<\/span><\/p>\n<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n

This procedure has been accredited at PICA since 2017 (DakkS).<\/p>\n

 <\/p>\n

Please contact us. We would be glad to inform you.<\/p>\n

Contact: Dr. Anna Romanotto (anna.romanotto@pica-berlin.de) or Tel.: +4930 255660062<\/p>\n","protected":false},"excerpt":{"rendered":"

The conventional method of determining pesticides in fats and oils (\u00a764 LFGB-Method Collection) L00.00-34) uses a complicated procedure to separate the pesticide molecules from the fat molecules. It is known as GPC (Gel Permeation Chromatography).\u00a0 After that, the large volume of solvent…
>> Read more<\/a><\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_relevanssi_hide_post":"","_relevanssi_hide_content":"","_relevanssi_pin_for_all":"","_relevanssi_pin_keywords":"","_relevanssi_unpin_keywords":"","_relevanssi_related_keywords":"","_relevanssi_related_include_ids":"","_relevanssi_related_exclude_ids":"","_relevanssi_related_no_append":"","_relevanssi_related_not_related":"","_relevanssi_related_posts":"","_relevanssi_noindex_reason":"","_genesis_hide_title":false,"_genesis_hide_breadcrumbs":false,"_genesis_hide_singular_image":false,"_genesis_hide_footer_widgets":false,"_genesis_custom_body_class":"","_genesis_custom_post_class":"","_genesis_layout":"","footnotes":""},"categories":[4,21],"tags":[],"class_list":{"0":"post-2573","1":"post","2":"type-post","3":"status-publish","4":"format-standard","6":"category-news","7":"category-research-and-development","8":"entry","9":"has-post-thumbnail"},"yoast_head":"\nhigh speed method for the determination of more than 700 pesticides in fat and oils - PiCA - Pr\u00fcfinstitut Chemische Analytik<\/title>\n<meta name=\"description\" content=\"The conventional method of determining pesticides in fats and oils (\u00a764 LFGB-Method Collection) L00.00-34) uses a complicated procedure to separate the\" \/>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/www.pica-berlin.de\/en\/news\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\/\" \/>\n<script type=\"application\/ld+json\" class=\"yoast-schema-graph\">{\"@context\":\"https:\\\/\\\/schema.org\",\"@graph\":[{\"@type\":\"Article\",\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/en\\\/news\\\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\\\/#article\",\"isPartOf\":{\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/en\\\/news\\\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\\\/\"},\"author\":{\"name\":\"Administrator\",\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/#\\\/schema\\\/person\\\/6919d389d5462abf2929600c621a93b7\"},\"headline\":\"high speed method for the determination of more than 700 pesticides in fat and oils\",\"datePublished\":\"2017-11-16T11:18:22+00:00\",\"dateModified\":\"2017-11-22T16:53:56+00:00\",\"mainEntityOfPage\":{\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/en\\\/news\\\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\\\/\"},\"wordCount\":255,\"publisher\":{\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/#organization\"},\"image\":{\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/en\\\/news\\\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\\\/#primaryimage\"},\"thumbnailUrl\":\"http:\\\/\\\/www.pica-berlin.de\\\/wp-content\\\/uploads\\\/2017\\\/11\\\/anna2.png\",\"articleSection\":[\"News\",\"research and development\"],\"inLanguage\":\"en-US\"},{\"@type\":\"WebPage\",\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/en\\\/news\\\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\\\/\",\"url\":\"https:\\\/\\\/www.pica-berlin.de\\\/en\\\/news\\\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\\\/\",\"name\":\"high speed method for the determination of more than 700 pesticides in fat and oils - PiCA - Pr\u00fcfinstitut Chemische Analytik\",\"isPartOf\":{\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/#website\"},\"primaryImageOfPage\":{\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/en\\\/news\\\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\\\/#primaryimage\"},\"image\":{\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/en\\\/news\\\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\\\/#primaryimage\"},\"thumbnailUrl\":\"http:\\\/\\\/www.pica-berlin.de\\\/wp-content\\\/uploads\\\/2017\\\/11\\\/anna2.png\",\"datePublished\":\"2017-11-16T11:18:22+00:00\",\"dateModified\":\"2017-11-22T16:53:56+00:00\",\"description\":\"The conventional method of determining pesticides in fats and oils (\u00a764 LFGB-Method Collection) L00.00-34) uses a complicated procedure to separate the\",\"breadcrumb\":{\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/en\\\/news\\\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\\\/#breadcrumb\"},\"inLanguage\":\"en-US\",\"potentialAction\":[{\"@type\":\"ReadAction\",\"target\":[\"https:\\\/\\\/www.pica-berlin.de\\\/en\\\/news\\\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\\\/\"]}]},{\"@type\":\"ImageObject\",\"inLanguage\":\"en-US\",\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/en\\\/news\\\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\\\/#primaryimage\",\"url\":\"http:\\\/\\\/www.pica-berlin.de\\\/wp-content\\\/uploads\\\/2017\\\/11\\\/anna2.png\",\"contentUrl\":\"http:\\\/\\\/www.pica-berlin.de\\\/wp-content\\\/uploads\\\/2017\\\/11\\\/anna2.png\"},{\"@type\":\"BreadcrumbList\",\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/en\\\/news\\\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\\\/#breadcrumb\",\"itemListElement\":[{\"@type\":\"ListItem\",\"position\":1,\"name\":\"Startseite\",\"item\":\"https:\\\/\\\/www.pica-berlin.de\\\/en\\\/\"},{\"@type\":\"ListItem\",\"position\":2,\"name\":\"high speed method for the determination of more than 700 pesticides in fat and oils\"}]},{\"@type\":\"WebSite\",\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/#website\",\"url\":\"https:\\\/\\\/www.pica-berlin.de\\\/\",\"name\":\"PiCA - Pr\u00fcfinstitut Chemische Analytik\",\"description\":\"\",\"publisher\":{\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/#organization\"},\"potentialAction\":[{\"@type\":\"SearchAction\",\"target\":{\"@type\":\"EntryPoint\",\"urlTemplate\":\"https:\\\/\\\/www.pica-berlin.de\\\/?s={search_term_string}\"},\"query-input\":{\"@type\":\"PropertyValueSpecification\",\"valueRequired\":true,\"valueName\":\"search_term_string\"}}],\"inLanguage\":\"en-US\"},{\"@type\":\"Organization\",\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/#organization\",\"name\":\"PiCA Pr\u00fcfinstitut Chemische Analytik GmbH\",\"url\":\"https:\\\/\\\/www.pica-berlin.de\\\/\",\"logo\":{\"@type\":\"ImageObject\",\"inLanguage\":\"en-US\",\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/#\\\/schema\\\/logo\\\/image\\\/\",\"url\":\"https:\\\/\\\/www.pica-berlin.de\\\/wp-content\\\/uploads\\\/2016\\\/06\\\/pica-pruefinstitut-chemische-analytik.gif\",\"contentUrl\":\"https:\\\/\\\/www.pica-berlin.de\\\/wp-content\\\/uploads\\\/2016\\\/06\\\/pica-pruefinstitut-chemische-analytik.gif\",\"width\":192,\"height\":103,\"caption\":\"PiCA Pr\u00fcfinstitut Chemische Analytik GmbH\"},\"image\":{\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/#\\\/schema\\\/logo\\\/image\\\/\"}},{\"@type\":\"Person\",\"@id\":\"https:\\\/\\\/www.pica-berlin.de\\\/#\\\/schema\\\/person\\\/6919d389d5462abf2929600c621a93b7\",\"name\":\"Administrator\"}]}<\/script>\n<!-- \/ Yoast SEO plugin. -->","yoast_head_json":{"title":"high speed method for the determination of more than 700 pesticides in fat and oils - PiCA - Pr\u00fcfinstitut Chemische Analytik","description":"The conventional method of determining pesticides in fats and oils (\u00a764 LFGB-Method Collection) L00.00-34) uses a complicated procedure to separate the","robots":{"index":"index","follow":"follow","max-snippet":"max-snippet:-1","max-image-preview":"max-image-preview:large","max-video-preview":"max-video-preview:-1"},"canonical":"https:\/\/www.pica-berlin.de\/en\/news\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\/","schema":{"@context":"https:\/\/schema.org","@graph":[{"@type":"Article","@id":"https:\/\/www.pica-berlin.de\/en\/news\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\/#article","isPartOf":{"@id":"https:\/\/www.pica-berlin.de\/en\/news\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\/"},"author":{"name":"Administrator","@id":"https:\/\/www.pica-berlin.de\/#\/schema\/person\/6919d389d5462abf2929600c621a93b7"},"headline":"high speed method for the determination of more than 700 pesticides in fat and oils","datePublished":"2017-11-16T11:18:22+00:00","dateModified":"2017-11-22T16:53:56+00:00","mainEntityOfPage":{"@id":"https:\/\/www.pica-berlin.de\/en\/news\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\/"},"wordCount":255,"publisher":{"@id":"https:\/\/www.pica-berlin.de\/#organization"},"image":{"@id":"https:\/\/www.pica-berlin.de\/en\/news\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\/#primaryimage"},"thumbnailUrl":"http:\/\/www.pica-berlin.de\/wp-content\/uploads\/2017\/11\/anna2.png","articleSection":["News","research and development"],"inLanguage":"en-US"},{"@type":"WebPage","@id":"https:\/\/www.pica-berlin.de\/en\/news\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\/","url":"https:\/\/www.pica-berlin.de\/en\/news\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\/","name":"high speed method for the determination of more than 700 pesticides in fat and oils - PiCA - Pr\u00fcfinstitut Chemische Analytik","isPartOf":{"@id":"https:\/\/www.pica-berlin.de\/#website"},"primaryImageOfPage":{"@id":"https:\/\/www.pica-berlin.de\/en\/news\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\/#primaryimage"},"image":{"@id":"https:\/\/www.pica-berlin.de\/en\/news\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\/#primaryimage"},"thumbnailUrl":"http:\/\/www.pica-berlin.de\/wp-content\/uploads\/2017\/11\/anna2.png","datePublished":"2017-11-16T11:18:22+00:00","dateModified":"2017-11-22T16:53:56+00:00","description":"The conventional method of determining pesticides in fats and oils (\u00a764 LFGB-Method Collection) L00.00-34) uses a complicated procedure to separate the","breadcrumb":{"@id":"https:\/\/www.pica-berlin.de\/en\/news\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\/#breadcrumb"},"inLanguage":"en-US","potentialAction":[{"@type":"ReadAction","target":["https:\/\/www.pica-berlin.de\/en\/news\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\/"]}]},{"@type":"ImageObject","inLanguage":"en-US","@id":"https:\/\/www.pica-berlin.de\/en\/news\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\/#primaryimage","url":"http:\/\/www.pica-berlin.de\/wp-content\/uploads\/2017\/11\/anna2.png","contentUrl":"http:\/\/www.pica-berlin.de\/wp-content\/uploads\/2017\/11\/anna2.png"},{"@type":"BreadcrumbList","@id":"https:\/\/www.pica-berlin.de\/en\/news\/high-speed-method-for-the-determination-of-more-than-700-pesticides-in-fat-and-oils\/#breadcrumb","itemListElement":[{"@type":"ListItem","position":1,"name":"Startseite","item":"https:\/\/www.pica-berlin.de\/en\/"},{"@type":"ListItem","position":2,"name":"high speed method for the determination of more than 700 pesticides in fat and oils"}]},{"@type":"WebSite","@id":"https:\/\/www.pica-berlin.de\/#website","url":"https:\/\/www.pica-berlin.de\/","name":"PiCA - Pr\u00fcfinstitut Chemische Analytik","description":"","publisher":{"@id":"https:\/\/www.pica-berlin.de\/#organization"},"potentialAction":[{"@type":"SearchAction","target":{"@type":"EntryPoint","urlTemplate":"https:\/\/www.pica-berlin.de\/?s={search_term_string}"},"query-input":{"@type":"PropertyValueSpecification","valueRequired":true,"valueName":"search_term_string"}}],"inLanguage":"en-US"},{"@type":"Organization","@id":"https:\/\/www.pica-berlin.de\/#organization","name":"PiCA Pr\u00fcfinstitut Chemische Analytik GmbH","url":"https:\/\/www.pica-berlin.de\/","logo":{"@type":"ImageObject","inLanguage":"en-US","@id":"https:\/\/www.pica-berlin.de\/#\/schema\/logo\/image\/","url":"https:\/\/www.pica-berlin.de\/wp-content\/uploads\/2016\/06\/pica-pruefinstitut-chemische-analytik.gif","contentUrl":"https:\/\/www.pica-berlin.de\/wp-content\/uploads\/2016\/06\/pica-pruefinstitut-chemische-analytik.gif","width":192,"height":103,"caption":"PiCA Pr\u00fcfinstitut Chemische Analytik GmbH"},"image":{"@id":"https:\/\/www.pica-berlin.de\/#\/schema\/logo\/image\/"}},{"@type":"Person","@id":"https:\/\/www.pica-berlin.de\/#\/schema\/person\/6919d389d5462abf2929600c621a93b7","name":"Administrator"}]}},"_links":{"self":[{"href":"https:\/\/www.pica-berlin.de\/en\/wp-json\/wp\/v2\/posts\/2573","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/www.pica-berlin.de\/en\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/www.pica-berlin.de\/en\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/www.pica-berlin.de\/en\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/www.pica-berlin.de\/en\/wp-json\/wp\/v2\/comments?post=2573"}],"version-history":[{"count":0,"href":"https:\/\/www.pica-berlin.de\/en\/wp-json\/wp\/v2\/posts\/2573\/revisions"}],"wp:attachment":[{"href":"https:\/\/www.pica-berlin.de\/en\/wp-json\/wp\/v2\/media?parent=2573"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/www.pica-berlin.de\/en\/wp-json\/wp\/v2\/categories?post=2573"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/www.pica-berlin.de\/en\/wp-json\/wp\/v2\/tags?post=2573"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}